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An investigation into the sample preparation procedure and analysis of cyanoacrylate adhesives using capillary electrophoresis

Whitaker, Gillian, Kincaid, Brendan J., van Hoof, Nicole, Regan, Fiona orcid logoORCID: 0000-0002-8273-9970, Smyth, Malcolm R. and Leonard, Raymond G. (2007) An investigation into the sample preparation procedure and analysis of cyanoacrylate adhesives using capillary electrophoresis. International Journal of Adhesion and Adhesives, 27 (7). pp. 604-609. ISSN 0143-7496

Abstract
In this study, the trace acid profile of cyanoacrylate adhesives was studied using capillary electrophoresis. Liquid–liquid extraction was employed as the sample preparation step before separation by capillary electrophoresis. The solubility of the adhesives was investigated using various organic solvents, e.g. hexane and dichloromethane, and chloroform was determined to be the optimum solvent as it enabled the full dissolution of the adhesive. A comprehensive stability study was performed over a 3-year period and results indicate that the adhesives were stable for 2 years after which their stability and performance degraded.
Metadata
Item Type:Article (Published)
Refereed:Yes
Uncontrolled Keywords:Cyanoacrylate; Capillary electrophoresis; Cure/hardening;
Subjects:Physical Sciences > Chemistry
DCU Faculties and Centres:DCU Faculties and Schools > Faculty of Science and Health > School of Chemical Sciences
Research Institutes and Centres > National Centre for Sensor Research (NCSR)
Publisher:Elsevier
Official URL:http://dx.doi.org/10.1016/j.ijadhadh.2006.11.001
Use License:This item is licensed under a Creative Commons Attribution-NonCommercial-Share Alike 3.0 License. View License
ID Code:151
Deposited On:21 Jan 2008 by DORAS Administrator . Last Modified 01 Jul 2019 15:42
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