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X-ray tomography, AFM and nanoindentation measurements for recyclability analysis of 316L powders in 3D printing process

Gorji, Nima E. orcid logoORCID: 0000-0002-1213-2364, O'Connor, Robert orcid logoORCID: 0000-0001-5794-6188 and Brabazon, Dermot orcid logoORCID: 0000-0003-3214-6381 (2020) X-ray tomography, AFM and nanoindentation measurements for recyclability analysis of 316L powders in 3D printing process. Procedia Manufacturing, 47 . pp. 1113-1116. ISSN 2351-9789

Abstract
Recyclability of the leftover metallic powder within the Additive manufacturing (3D printing) process has been less systematically investigated by the research groups although it is a usual practice in most academic and industrial laboratories to reuse the leftover powders for subsequent printing cycles. A better understanding of these mechanisms will assist in optimizing the number of times the recycled powder can be reused in the process to reduce the powder waste. We have recently focused on characterization of recycled powders left in the powder bed after the powder bed fusion process and evaluated the extent of porosity in the powder particles. X-ray computing tomography technique (XCT) has been used to analyze the concentration of porosity, inclusions and dendrites induced inside the recycled powder particles and compared that to the fresh counterparts. The XCT resolution of 2 m was set to separately scan the powder badges for 3 hours. A roughly 10% more porosity has been calculated in reused powder particles (in at least 10 times reused power). Atomic Force Microscopy (AFM) was used to measure the roughness of the surface of powder particles which shows average roughness of 4.29 nm and 5.49 nm for the virgin and recycled powders, respectively. Nanoindentation measurement were also applied on a number of locations of the particles to compare the hardness of the virgin and recycled powders. For example, the recycled powder shows smaller a hardness of 207 GPa and an effective modulus of 9.60 GPa (average values) compared to 237 GPa and 9.87 GPa (average values) for it’s virgin counterpart which can be correlated to porosities created beneath the surface. Nanoindentation was also applied on (micro and nano) polished surface of the particles under a force of 250 N for up to 10 seconds. The stainless Steel 316L powder has been the material under study with the powder particles of average size 50 m which were analyzed using Xradia XCT, Bruker Dimension ICON AFM and Bruker HYSITRON TI Nanoindentation systems. Further investigation is ongoing to correlate the mechanical properties of the manufactured parts to the microstructure and chemical compositions of the virgin and recycled powders.
Metadata
Item Type:Article (Published)
Refereed:Yes
Uncontrolled Keywords:Additive Manufacturing; 3D Printing; Powders Recycling; AFM; X-ray Computing; Tomography; Nanoindentation
Subjects:Engineering > Materials
Engineering > Mechanical engineering
Engineering > Production engineering
DCU Faculties and Centres:DCU Faculties and Schools > Faculty of Engineering and Computing > School of Mechanical and Manufacturing Engineering
Research Institutes and Centres > Advanced Processing Technology Research Centre (APT)
Research Institutes and Centres > I-Form
Publisher:Elsevier
Official URL:https://dx.doi.org/10.1016/j.promfg.2020.04.127
Copyright Information:© 2020 The Authors.
Funders:SFI
ID Code:26104
Deposited On:11 Aug 2021 12:45 by Dermot Brabazon . Last Modified 28 Nov 2023 12:10
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