Ferguson, George, Gallagher, John F. 
ORCID: 0000-0002-7112-7450, Murphy, Denis, Spalding, Trevor R., Glidewell, Christopher and Holden, H. Diane
(1992)
The structure of triphenylgermanium hydroxide.
Acta Crystallographica Section C, 48
(7).
pp. 1228-1231.
ISSN 0108-2701
Abstract
C18H~6GeO, Mr = 320.9, triclinic, Pi, a =
15.408 (6), b = 19.974 (7), c = 23.264 (11) A, a =
107.78 (4), 13 = 1.03.54 (4), y= 101.51 (3) °, V =
6338 (5)/~3, Z = 16, Dx = 1.34 g cm -3, a(Mo Ka) =
0.71073A, /z = 19.1cm-1, F(000)=2624, T=
293 K, R = 0.055 for 6846 observed reflections. The
eight independent molecules in the asymmetric unit
form two independent O--H...O hydrogen-bonded
tetramers with the O atoms in a flattened tetrahedral
arrangement [hydrogen-bond distances in the range
2.609 (11) to 2.657 (11)A]. The Ge atoms are tetrahedrally
coordinated with mean Gc O 1.791 (7) and
Gc C 1.931 (8) A.
Metadata
| Item Type: | Article (Published) |
|---|---|
| Refereed: | Yes |
| Subjects: | Physical Sciences > Organic chemistry Physical Sciences > Crystallography |
| DCU Faculties and Centres: | DCU Faculties and Schools > Faculty of Science and Health > School of Chemical Sciences |
| Publisher: | International Union of Crystallography |
| Official URL: | http://dx.doi.org/10.1107/S0108270191015056 |
| Copyright Information: | © 1992 International Union of Crystallography |
| Use License: | This item is licensed under a Creative Commons Attribution-NonCommercial-Share Alike 3.0 License. View License |
| ID Code: | 3611 |
| Deposited On: | 18 Mar 2009 17:18 by DORAS Administrator . Last Modified 10 Oct 2018 12:52 |
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